Characterisation of polyester resins and composites by differential scanning calorimetry (DSC) and thermogravimetry (TG)

D. Singh, A. K. Govila, V.K. Ganpate
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Abstract

Polyester resins and their composite have been evaluated by using two of the thermoanalytical methods viz. Differential Scanning Calorimetry (DSC) and Thermo gravimetry (TG). With the help of DSC, data on state of “B” stage cure, optimum curing temperature was obtained for a polyester resin and Dough Moulding compounds obtained from two different source. These results helped to optimise process parameters. Thermogravimetry has been used to determine heat resistance of polyester resins and DMC composites. Energy oh activation for degradation process has also been calculated which resembles closely with theoretical values. In this Paper, the methodology of experimentation and the results obtained have been discussed which elucidate the importance of using thermo analytical methods for quick and reliable results.
差示扫描量热法(DSC)和热重法(TG)表征聚酯树脂和复合材料
采用差示扫描量热法(DSC)和热重法(TG)两种热分析方法对聚酯树脂及其复合材料进行了评价。利用DSC,对两种不同来源的聚酯树脂和面团成型化合物的B段固化状态、最佳固化温度进行了分析。这些结果有助于优化工艺参数。热重法用于测定聚酯树脂和DMC复合材料的耐热性。还计算了降解过程的活化能,结果与理论值非常接近。本文讨论了实验方法和所得结果,说明了采用热分析方法获得快速可靠结果的重要性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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