Analysis of organophosphorus pesticide residues in selected vegetables purchased from Narsingdi district of Bangladesh using QuEChERS Extraction

Nuzat Tasnim, Md Nasrul Millat, Sadia Sultana, S. Rahman, M. Prodhan
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引用次数: 4

Abstract

Pesticide residues in different crops, including food grains and vegetables are burning issues in Bangladesh. Therefore, the present study was conducted to analyze organophosphorus pesticide residues in three popular vegetables (cauliflower, hyacinth bean and yard long bean) collected from five local markets of Narsingdi district of Bangladesh. The collected vegetable samples were extracted and cleaned up using Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) extraction technique and analyzed by Gas Chromatography (GC) equipped with Flame Thermionic Detector (FTD). A total of 45 vegetable samples were analyzed. Among the 15 analyzed samples of hyacinth bean, three samples (20 % of the total samples) contained pesticide residues above the EU-MRL and the remaining samples did not contain any detectable residues of the selected organophosphorus pesticides. In case of  cauliflower, out of 15 analyzed samples, two samples (13% of the total number of samples) contained pesticide residues above the EU-MRL. In case of yard long bean, of the 15 analyzed samples, four samples (27% of the total number of samples) contained pesticide residues above the EU-MRLs. This study reveals the present status of pesticide residue contamination in the selected vegetables. Asian Australas. J. Biosci. Biotechnol. 2022, 7 (3), 114-121
采用QuEChERS萃取法对孟加拉国纳辛格迪地区所购蔬菜中的有机磷农药残留进行了分析
包括粮食和蔬菜在内的不同作物中的农药残留是孟加拉国亟待解决的问题。因此,本研究对从孟加拉国Narsingdi区5个当地市场采集的3种常见蔬菜(花椰菜、风信子豆和院子长豆)中的有机磷农药残留进行了分析。采用快速、简便、廉价、有效、坚固、安全(QuEChERS)提取技术对蔬菜样品进行提取和清洗,并采用配备火焰热离子检测器(FTD)的气相色谱(GC)进行分析。共分析了45份蔬菜样品。在15个风信子豆分析样品中,3个样品(占总样品的20%)的农药残留量高于EU-MRL,其余样品未检测到所选有机磷农药的残留。以花椰菜为例,在分析的15个样品中,有两个样品(占样品总数的13%)的农药残留高于欧盟最大残留限量。就菜豆而言,在15个分析样本中,有4个样本(占样本总数的27%)的农药残留超过欧盟最大残留限量。本研究揭示了所选蔬菜中农药残留污染的现状。亚洲Australas。j . Biosci。生物工程学报,2016,37 (3),394 - 394
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