Influence of temperature on microstructure and electrical properties of znic doped CCTO ceramics

Dong-yu Xu, Yan Zhao, Song Bai, Yuanling Liu, H. Ding
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Abstract

The influence of sintering temperature on microstructure and electrical properties of Zn doped CaCu3Ti4O12 ceramics were investigated. The CaCu3−xZnxTi4O12 (x=0, 0.06, 0.1, 0.2) ceramics were prepared by sol-gel method, and sintered at 950 □, 1000 □, 1050 □, 1100 □. XRD patterns confirm the formation of CCTO crystal phase in the as-prepared samples, and SEM results showed different porous structures and grain sizes at different temperatures. The results were commented and discussed on the temperature effect on electric properties and microstructure of CaCu3−xZnxTi4O12 ceramics.
温度对掺杂锌CCTO陶瓷微观结构和电性能的影响
研究了烧结温度对掺锌cuu3ti4o12陶瓷微观结构和电学性能的影响。采用溶胶-凝胶法制备了CaCu3−xZnxTi4O12 (x= 0,0.06, 0.1, 0.2)陶瓷,并在950□,1000□,1050□,1100□下进行了烧结。XRD图证实了制备样品中CCTO晶相的形成,SEM结果显示不同温度下的多孔结构和晶粒尺寸不同。讨论了温度对cucu3−xZnxTi4O12陶瓷电性能和微观结构的影响。
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